The crystal structure of 3,3′-disulfanediyldi(1<i>H</i>-1,2,4-triazol-5-amine) monohydrate, C<sub>4</sub>H<sub>8</sub>N<sub>8</sub>OS<sub>2</sub>
نویسندگان
چکیده
Abstract C 4 H 8 N OS 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.4377(5) Å, b 7.5032(5) c 10.0964(6) α 91.481(5)°, β 108.906(5)°, γ 110.678(6)°, V 492.41(6) Å 3 Z 2, R gt ( F ) 0.0653, wR ref 0.1888, T 293 (2) K.
منابع مشابه
3-Phenyl-1H-1,2,4-triazol-5-amine–5-phenyl-1H-1,2,4-triazol-3-amine (1/1)
In the title compound, C(8)H(8)N(4)·C(8)H(8)N(4), two tautomers, viz. 3-phenyl-1,2,4-triazol-5-amine and 5-phenyl-1,2,4-triazol-3-amine, are crystallized together in equal amounts. The 3-phenyl-1,2,4-triazol-5-amine mol-ecule is essentially planar; the phenyl ring makes a dihedral angle of 2.3 (2)° with the mean plane of the 1,2,4-triazole ring. In the 5-phenyl-1,2,4-triazol-3-amine tautomer, t...
متن کامل3,5-Bis(4-hydroxyphenyl)-4H-1,2,4-triazol-4-amine monohydrate
The triazole ring in the title compound, C(14)H(12)N(4)O(2)·H(2)O, makes dihedral angles of 36.9 (1) and 37.3 (1)° with the two benzene rings. Each hy-droxy group is a hydrogen-bond donor to a two-coordinate N atom of an adjacent mol-ecule; these O-H⋯N hydrogen bonds generate a layer parallel to the ab plane. Adjacent layers are linked by N--H⋯O and O(water)-H⋯O hydrogen bonds into a three-dime...
متن کامل3-Benzylsulfanyl-1H-1,2,4-triazol-5-amine
In the title mol-ecule, C(9)H(10)N(4)S, the dihedral angle between the benzene and triazole rings is 81.05 (5)°. In the crystal, N-H⋯N hydrogen bonds link the mol-ecules into infinite zigzag chains along [010].
متن کاملCrystal structure of N-(2-hydroxyethyl)-5-nitroisophthalamic acid monohydrate
In the title compound, C10H10N2O6·H2O, the carb-oxy-lic acid group and the nitro group are essentially coplanar with the benzene ring [maximum deviation = 0.0264 (9) Å], while the amide group is oriented at a dihedral angle of 9.22 (5)° with respect to the benzene ring. In the crystal, classical O-H⋯O and N-H⋯O hydrogen bonds and weak C-H⋯O inter-actions link the organic mol-ecules and water mo...
متن کامل3-Pyridin-2-yl-1H-1,2,4-triazol-5-amine
In the title compound, C(7)H(7)N(5), the non-H atoms are almost coplanar (r.m.s. deviation = 0.050 Å), with the N atom of pyridine ring oriented to the N-N(H) side of the 1,2,4-triazole ring. The mean planes of the pyridine and 1,2,4-triazole rings form a dihedral angle of 5.58 (7)°. The N atom of the amino group adopts a pyramidal configuration. The mol-ecules are linked into a two-dimensional...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Zeitschrift Fur Kristallographie-new Crystal Structures
سال: 2022
ISSN: ['2197-4578', '1433-7266']
DOI: https://doi.org/10.1515/ncrs-2022-0519